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Ultrasonic-assisted synthesis of starch-stabilized silver nanoparticles

MOHAMMAD HAKIMI1, MAJID DARROUDI2,* , ALI KHORSAND ZAK3, MUHAMAD RASAT MUHAMAD4, HASAN ALI HOSSEINI1

Affiliation

  1. Chemistry Department, Payame Noor University, 19395-4697, Tehran, Iran
  2. Department of Modern Sciences and Technologies, School of Medicine, Mashhad University of Medical Sciences, Mashhad, Iran
  3. Low Dimensional Materials Research Center, Department of Physics, Faculty of Science, University of Malaya, 50603, Kuala Lumpur, Malaysia
  4. Chancellery, University of Multimedia, Cyberjaya Campus, 63100 Cyberjaya, Selangor, Malaysia

Abstract

Well-dispersed and uniform starch-stabilized silver nanoparticles (Ag-NPs) with a relatively narrow size distribution are prepared via green chemistry method by ultrasonic procedure. Solutions containing silver ions and starch in water gave starch-capped Ag-NPs, which could be integrated into medical applications such as using in antibacterial wound dressing. Eco-friendly materials as bio-organisms in plant extracts contain polysaccharides, which act as both reducing and capping agents forming stable and size-controlled Ag-NPs. The size of the Ag-NPs decreases with the ultrasonic time. Ultrafine spherical Ag-NPs with a mean particle size of about 8.5 nm have been synthesized under ultrasonic process. X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), UV–Vis spectroscopy, and transmission electron microscopy (TEM) are used to characterize the starch-stabilized Ag-NPs..

Keywords

Silver nanoparticles, Starch, Ultrasonic irradiation, Green chemistry.

Citation

MOHAMMAD HAKIMI, MAJID DARROUDI, ALI KHORSAND ZAK, MUHAMAD RASAT MUHAMAD, HASAN ALI HOSSEINI, Ultrasonic-assisted synthesis of starch-stabilized silver nanoparticles, Optoelectronics and Advanced Materials - Rapid Communications, 6, 9-10, September-October 2012, pp.840-843 (2012).

Submitted at: May 30, 2012

Accepted at: Sept. 20, 2012