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Synthesis and characterization on hydro phobic monomer 4-butyl styrene

MA CHAO1,2,* , LIU QIAO3, ZHANG XI4, WAN GANG5, LI LUN6

Affiliation

  1. College of Petroleum Engineering , Yangtze University , Province Key Laboratory of Oil and Gas Drilling and Production Engineering Wuhan 430100, Hubei, China
  2. The State Key Laboratory of Polymer Materials Engineering , Polymer Research Institute of Sichuan University, Chengdu 610065 , S ichuan, China
  3. The State Key Laboratory of Polymer Materials Engineering , Polymer Research Institute of Sichuan University, Chengdu 610065, Sichuan, China
  4. The State Key Laboratory of Polymer Materials Engineering , Polymer Research Institute of Sichuan University , Chengdu 610065 , S ichuan, China
  5. College of Petroleum Engineering, Yangtze University , Province Key Laboratory of Oil and Gas Drilling and Production Engineering Wuhan 430100 , Hubei , China
  6. College of Petroleum Engineering, Yangtze University , Province Key Laboratory of Oil and Gas Drilling and Production Engineering Wuhan 430100, Hubei, China

Abstract

4-butyl styrene has a good copolymerization activity with acrylamide. Benzene can i mprove rigidity of copolymer molecular and meanwhile benzene which is hydrophobic group, can not only enhance the thermal resistance and salt tolerance, but also produce hydrophobic association for copolymer. This paper describes how to prepare hydrophobic monomer 4 butyl styrene from butylbenzene by Friedel Crafts Acylation Reaction, hydrogen transfer reduction, dehydration of the alcohol to alkene. Product is studied as 4 butyl styrene with high purity through IR, 1HNMR..

Keywords

4-butyl styrene, Hydrophobic monomer, Micellar copolymerization, Temperature sensitive polymer.

Citation

MA CHAO, LIU QIAO, ZHANG XI, WAN GANG, LI LUN, Synthesis and characterization on hydro phobic monomer 4-butyl styrene, Optoelectronics and Advanced Materials - Rapid Communications, 10, 3-4, March-April 2016, pp.232-235 (2016).

Submitted at: Dec. 18, 2014

Accepted at: April 5, 2016