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Hydrothermal assisted synthesis followed by reduction route: Gd2O2S:Eu3+ hollow spheres and their photoluminescence properties

HUILIN QU1, JINGBAO LIAN1,* , HUA QIN1, NIANCHU WU1, XUE ZHANG1, JIAO HE1

Affiliation

  1. School of Mechanical Engineering, Liaoning Petrochemical University, Fushun, 113001, P.R. China

Abstract

Herein, a homogeneous Gd2O2S:Eu3+ hollow spheres with pure phase structure were synthesized successfully through the calcination and reduction of the precursors prepared by hydrothermal method. It’s worth noting that the non-template method is used to replace the traditional template method in this paper. The optimum calcination temperature of the precursor is 800 oC. FE-SEM and TEM observation indicate the target products are hollow spheres with a size range of 200-400 nm. When the doping concentration of Eu3+ is 7.50%, the luminescence intensity is the highest and its CIE coordinate fluorescence lifetime are (0.629, 0.370) and 1.114 μs.

Keywords

Rare earth luminescent materials, Gadolinium oxysulfide, Hollow spheres, Reduction route, Photoluminescence.

Citation

HUILIN QU, JINGBAO LIAN, HUA QIN, NIANCHU WU, XUE ZHANG, JIAO HE, Hydrothermal assisted synthesis followed by reduction route: Gd2O2S:Eu3+ hollow spheres and their photoluminescence properties, Optoelectronics and Advanced Materials - Rapid Communications, 16, 7-8, July-August 2022, pp.348-358 (2022).

Submitted at: Jan. 11, 2022

Accepted at: Aug. 10, 2022