Our site saves small pieces of text information (cookies) on your device in order to deliver better content and for statistical purposes. You can disable the usage of cookies by changing the settings of your browser. By browsing our site without changing the browser settings you grant us permission to store that information on your device.
K. KANAGASABAPATHY1,* , S. VETRIVEL2, R. RAJASEKARAN2
Tristhiourea Zinc(II)Sulphate(ZTS) and L-Arginine added Tristhiourea Zinc(II)Sulphate compounds were synthesized and single crystals were grown by slow evaporation technique. The cell parameters of the grown crystals were evaluated by single crystal X-ray diffraction technique. The powder X-ray diffraction patterns were recorded and indexed for further confirmation of crystalline nature of grown crystals. The crystalline perfection has been identified by etching studies. The presence of functional groups in the crystals has been confirmed by FTIR analysis. UV-Visible absorption spectra have been recorded to find the cutoff wavelength of the grown crystals. TGA/DTA and DSC studies show the thermal behavior of the grown crystals. The microhardness studies on the crystal samples revealed that the hardness increases with applied load for all the grown crystals. From the values of work hardening coefficient, it is found that ZTS and L-Arginine added ZTS crystals belong to the soft category materials. The second harmonic generation in the grown crystals was confirmed by Kurtz Perry powder method using Nd:YAG laser..
Growth from solution, X-ray diffraction, FTIR, Nonlinear material, Second Harmonic Generation.
K. KANAGASABAPATHY, S. VETRIVEL, R. RAJASEKARAN, Growth, structural, optical, hardness and thermal studies of L-Arginine added TrisThiourea Zinc(II)Sulphate single crystals, Optoelectronics and Advanced Materials - Rapid Communications, 6, 11-12, November-December 2012, pp.1118-1123 (2012).
Submitted at: June 10, 2012
Accepted at: Oct. 30, 2012
Optoelectronics and Advanced Materials - Rapid Communications
(2022): 0.5 - 2022 Journal Citation Reports (Clarivate Analytics, 2023)
Active accounts were imported to the new platform and assigned a random password by default. In order to access your account you need to access the login page and go through the Lost Password dialog (involves the system sending you an email with instructions) in order to reset your password. This step is necessary as passwords are kept in hashed form and the new platform uses modern hashing algorithms incompatible with the previous ones.